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(d) To understand why the Br atom is abstracted, we must realize that bromine is less electronegative than oxygen. Therefore the LUMO which is the sBrO orbital is polarized toward Br. Since the alkyl radical SOMO is high in energy (i.e., at ), the SOMO LUMO interaction will be more important than any interaction with the occupied orbitals. 15. Reductive decyanations of 2-cyanotetrahydropyran derivatives with sodium in ammonia yield predominantly axially protonated products. The observations are consistent with the reductive decyanation proceeding via the pyramidal, axial radical which accepts a second electron to give a con gurationally stable carbanion, which in turn abstracts a proton from ammonia with retention of con guration (Rychnovsky, S. D.; Powers, J. P.; LePage, T. J., J. Am. Chem. Soc., 1992, 114, 8375 8384). Provide an explanation for the axial preference of the intermediate free radical on the basis of orbital interactions. Hint: The title of the paper by Rychnovsky et al. is ``Conformation and Reactivity of Anomeric Radicals.''

R y F1 N; N; 1 2N 1 R 1 R N 1 !

Communities naturally form around shared interests, whether they are defined by ethical or political values, geographic region, or type of activity (see Exhibit 7.3). In today s online world, there is extensive competition for audience attention in both

Figure 29-22: Anchoring the Products Design site to the anchor or page to which it will connect within the existing site Figure 29-23: The would-be Products section of the site is successfully anchored into the existing site as a sibling to the Services section of the site. It is now ready to have children.

DR Navigation DR navigation is the method of deducing your position using only heading steered and distance run. This is deduced navigation and is often known, erroneously in my opinion, as dead reckoning rather than ded. reckoning , but anyway it s commonly called DR . If you know where you started from, the direction in which the boat has been travelling and the distance travelled, it s very easy to plot where you are on a chart. This makes no allowance for tide or wind, so is only of use in relatively calm conditions where there is little or no tide.

SELECT ename FROM emp WHERE NOT (sal=2975 OR comm=500)

The trick is to get the screw out without opening the PSU, because this can void your warranty, but more seriously is that it can hold a charge after being disconnected from the electrical supply a charge that s got enough power to kill you. Lucky thing is that if the screw went in, you should be able to get it out the same way. It s not going to be easy, but with some precision shaking you will either get it out or get it to a point where you can use pliers to grab it.

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The archive manager module provides the following functionalities:

Turn off the Ignore Palettes check box on the Options bar if you want Photoshop to stop resizing the window when the window bumps up against a palette that s anchored against the side of the program window. Turn the option on to resize the window regardless of the palettes. The palettes then float over the resized window. To access the zoom tool temporarily when some other tool is selected, press and hold the Ctrl and spacebar keys. Release both keys to return control of the cursor to the selected tool. To access the zoom out cursor, press Alt with the spacebar. These keyboard equivalents work from inside many dialog boxes, enabling you to modify the view of an image while applying a filter or color correction.

Lights can be difficult to select; they may be inside a lamp or high up, out of your current display. Distant lights don t have a glyph that you can click on to select them. The List in Model palette helps you select, modify, and delete lights. To select a light, choose it in the palette. You can now edit the light either with grips or in the Properties palette. Figure 25-7 shows a selected spotlight. You can easily change the spotlight s location, target, hotspot, and falloff using grips. To change its status (on or off), color, and other properties, use the Properties palette. To delete a light, choose it in the Lights in Model palette and press Del. You don t delete the sun, you just turn it off. (Good night!).

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